Three wheat samples collected in 1987 in Central Poland and naturally infected withFusarium spp were analyzed for the presence ofFusarium spp andFusarium toxins. Heads were separated into three fractions: kernels with visibleFusarium damage, healthy looking kernels, and chaff + rachis.The samples contained deoxynivalenol (2.0 - 40.0μg/g), nivalenol (O.O1μg/g), 4,7-dideoxynivalenol (0.10 - 0.15μg/g). 15-acetyldeoxynivalenol (0.10-2.00 μg/g), 3-acetyldeoxynivalenol (O/1Oμg/g), and zearalenone (0.01-2.00μg/g).This is the first report about 15 - acetyldeoxynivalenol in European wheat and the co-occurrence of 3 - acetyldeoxynivalenol and 15-acetyldeoxynivalenol in the same sample of contaminated cereals.