
doi: 10.1007/bf02646566
We have carried out a systematic experimental study of fracture in materials which contain hard second phase particles. The principal variables in this study were the average size and spacing of the second phase particles, grain size, temperature, and the strain rate. Polycrystalline copper containing a dispersion of silica particles was the material used in these experiments. Three modes of fracture were observed: transgranular necking fracture, fracture by the propagation of intergranular cracks initiated at the surface, and intergranular fracture by grain boundary cavitation throughout the entire specimen cross-section. The transition between the fracture modes was shown to shift systematically with temperature, strain rate, and the microstructure. The intergranular fracture mode was studied in detail. The growth of cavities in the grain boundaries was determined to be the rate limiting step in the fracture process. It was determined that in the range of 10-4 to 10-7 s-1 in strain rate, the dominant growth mechanism of the cavities was power-law creep rather than diffusional transport. The ductility of the material in the intergranular mode of fracture was found to be strongly dependent on the area fraction of the second phase in the grain boundary and on the strain rate sensitivity of the material; it was weakly dependent on the grain size. A theoretical lower bound and a practical upper bound of the ductility in the intergranular fracture mode were established. The results are in qualitative agreement with the data on nickel-base alloys and other materials published in the literature.
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