Purification of campesterol and preparation of 7‐dehydrocampesterol, 7‐campestenol and campestanol
Copyright policy )Purification of campesterol and preparation of 7‐dehydrocampesterol, 7‐campestenol and campestanol
AbstractCampesterol ([24R]‐24‐methyl‐5‐cholesten‐3β‐ol) was isolated from a soybean sterol mixture and purified on a small scale by column chromatography and on a large scale by crystallization from acetone to 97% purity. From this, 7‐dehydrocampesterol ([24R]‐24‐methyl‐5,7‐cholestadien‐3β‐ol) and campestanol ([24R]‐24‐methyl‐cholestan‐3β‐ol) were prepared. The acetates and benzoates of all four compounds also were obtained and compared to the corresponding members of the ergostane series.
- University of Arizona United States
Chromatography, Sterols, Chromatography, Gas, Glycine max, Cholestenes, Stigmasterol, Phytosterols, Chromatography, Thin Layer, Acetates, Benzoates, Sitosterols
Chromatography, Sterols, Chromatography, Gas, Glycine max, Cholestenes, Stigmasterol, Phytosterols, Chromatography, Thin Layer, Acetates, Benzoates, Sitosterols
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