Synthese von 22,26-Imino-cholestan-Derivaten

descriptionPublicationkeyboard_double_arrow_right Article 01 Nov 1961 German Publisher:Springer Science and Business Media LLCJournal:Experientia, volume 17, pages 490-491 (issn: 0014-4754, eissn: 1420-9071,

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Authors: K. Schreiber; G. Adam;

doi: 10.1007/bf02158612

Synthese von 22,26-Imino-cholestan-Derivaten

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Abstract

3β, 16α-diacetoxy-5α-pregnane-20-one and the analogue pregn-5-ene derivative have been converted into (22R, 25R)-22, 26-imino-5α-cholestane-3β, 16α-diol. The configuration at C-22 and C-25 was determined by transformation into the known (22R, 25R)-5α-solanidane-3-one. Application of the Ruschig method led to (25R)-22,26-imino-5α-cholest-22(N)-ene-3β, 16α-diol.

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