Modulated Differential Scanning Calorimetry

descriptionPublicationkeyboard_double_arrow_right Article 01 Dec 1997 English Publisher:Springer Science and Business Media LLCJournal:Journal of Thermal Analysis, volume 50, pages 727-744 (issn: 0368-4466,

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Authors: F. Cser; F. Rasoul; E. Kosior;

doi: 10.1007/bf01979203

Modulated Differential Scanning Calorimetry

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Abstract

The reproducibility and reliability of the TA Instruments Modulated Differential Scanning Calorimeter (MDSC) was tested over a range of conditions. The equipment base line was found to be fairly constant with a very small fluctuation (10 μW), which means a 0.1 % fluctuation on the scale of a normal polymer MDSC curve. The excellent stability of the base line and the reasonable reproducibility of the curves (5%) suggest that frequent calibration is not required.

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