Certified reference materials for thermal analysis
Copyright policy )Certified reference materials for thermal analysis
Eight inorganic substances recommended by ICTA as temperature standard reference materials for DTA and DSC were studied: KNO3, KClO4, Ag2SO4, K2CrO4, quartz, K2SO4, BaCO3 and SrCO3. The content of pure component in each of these substances was determined by classical chemical analysis. The temperatures and the heats of polymorphic transformations of these substances were measured with a Perkin-Elmer DSC-2 differential scanning calorimeter, and DTA studies were performed on a MOM 1500 D Q-derivatograph. The plot heat of transformation by DSCvs. DTA peak area is advanced as a calibration line for the approximate estimation of quantitative DTA effects. The substances studied will be certified as temperature standard reference materials for use in DTA and DSC.
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