Anodic stripping voltammetry of copper and bismuth

descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 1975 English Publisher:Springer Science and Business Media LLCJournal:Mikrochimica Acta, volume 63, pages 125-131 (issn: 0026-3672, eissn: 1436-5073,

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Authors: Atsushi Mizuike; Tomoo Miwa; Yukio Fujii;

doi: 10.1007/bf01271529

Anodic stripping voltammetry of copper and bismuth

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Abstract

Microgram and nanogram quantities of copper and bismuth are electrodeposited on a glassy carbon electrode from 10M hydro-fluoric-1M nitric acid solutions. The deposit is then anodically removed in 0.1M perchloric acid or 0.1–12M hydrochloric acid, a current-voltage curve being recorded. Copper and bismuth at p. p. b. levels in sponge zirconium are determined by this technique with 5 M hydrochloric acid as stripping electrolyte within 3 hours.

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Nagoya University
Japan

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