1H and13C NMR analysis of some trichothecenes

descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 1989 English Publisher:Springer Science and Business Media LLCJournal:Archives of Environmental Contamination and Toxicology, volume 18, pages 365-373 (issn: 0090-4341, eissn: 1432-0703,

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Authors: M, Mesilaakso; M, Moilanen; E, Rahkamaa;

doi: 10.1007/bf01062361

pmid: 2730157

1H and13C NMR analysis of some trichothecenes

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Abstract

1H and 13C NMR chemical shifts were determined from the NMR spectra of low concentration solutions of T-2 toxin, T-2 triol, HT-2 toxin, diacetoxyscirpenol, and neosolaniol. Isomerization of neosolaniol was observed to occur in chloroform solution. 1D and 2D 1H and 13C NMR techniques were used in order to determine the structure of the isomerization product, finally identified as 4 beta, 8 alpha-diacetoxy-3 alpha, 15-dihydroxy-12,13-epoxytrichothec-9-ene.

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Keywords

Carbon Isotopes, Chemistry, Magnetic Resonance Spectroscopy, Chemical Phenomena, Trichothecenes, Sesquiterpenes

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