Complexes of manganese borohydride with the borohydrides of organic cations

descriptionPublicationkeyboard_double_arrow_right Article 01 Feb 1989 English Publisher:Springer Science and Business Media LLCJournal:Bulletin of the Academy of Sciences of the USSR Division of Chemical Science, volume 38, pages 377-382 (issn: 0568-5230, eissn: 1573-9171,

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Authors: V. D. Makhaev; A. P. Borisov; T. P. Karpova; �. B. Lobkovskii; B. P. Tarasov; A. N. Chekhlov;

doi: 10.1007/bf00953633

Complexes of manganese borohydride with the borohydrides of organic cations

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Abstract

1. Reaction of MnCBH4)2(THF)3 with tetrabutylammoniura and tetraphenylphosphonium borohydndes, and with tetraphenylphosphonium chloride, has given the compounds (Bu4N)[Mn(BH4)3], (Ph4P)[Mn(BH4)3], (Ph4P)[Mn(BH4)3(THF)], (Ph4P) [Mn(BH4)3Cl], and (Ph4P) [Mn(BH4)2Cl(THF)], which have been characterized by IR spectroscopy and thermogravimetric studies. 2. The crystal and molecular structure of the manganese complex (Ph4P) [Mn(BH4)3−xClx (THF)] (x∼ 0.5) has been found.

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Russian Academy of Sciences
Russian Federation

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