Synthesis of aromatic compounds of types ArCH2CH = CCl2 and Ar?(CH2CH = CCl2)2

descriptionPublicationkeyboard_double_arrow_right Article 01 Apr 1959 English Publisher:Springer Science and Business Media LLCJournal:Bulletin of the Academy of Sciences of the USSR Division of Chemical Science, volume 8, pages 624-628 (issn: 0568-5230, eissn: 1573-9171,

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Authors: R. Kh. Freidlina; N. A. Semenov; A. N. Nesmeyanov;

doi: 10.1007/bf00915855

Synthesis of aromatic compounds of types ArCH2CH = CCl2 and Ar?(CH2CH = CCl2)2

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Abstract

1. The condensation of 1,1,3-trichloro-1-propene with benzene, toluene, 3-phenyl-1,1-dichloro-1-propene, 3-(p-chlorophenyl)-1,1-dichloro-1-propene, naphthalene and 3-phenyl-1,1,1,2-tetrachloropropane was carried out in the presence of aluminum chloride or antimony pentachloride, with the formation of the corresponding mono- and di-alkylated products. 2. α-chloro-p-chlorohydrocinnamic acid was prepared in good yield by the action of chlorine on 3-(p-chlorophenyl)-1, 1-dichloro-1-propene in concentrated sulfuric acid.

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Russian Academy of Sciences
Russian Federation

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