Synthesis of nitroalkyl-N-nitrosamines

descriptionPublicationkeyboard_double_arrow_right Article 01 Nov 1971 English Publisher:Springer Science and Business Media LLCJournal:Bulletin of the Academy of Sciences of the USSR Division of Chemical Science, volume 20, pages 2,480-2,482 (issn: 0568-5230, eissn: 1573-9171,

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Authors: R. G. Gafurov; E. M. Sogomonyan; L. T. Eremenko;

doi: 10.1007/bf00854346

Synthesis of nitroalkyl-N-nitrosamines

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Abstract

1. Nitroalkylamines of variable structure were nitrosated by nitrous acid and its chloro- and fluoro-derivatives. On the example of 1,1,1,6,6,6-hexanitro-3-azapentane it was shown that weakly basic amines do not react with ClNO in nonpolar organic solvents. 2. The obtained nitroalkyl-N-nitrosamines are smoothly converted to N-nitramines by treatment with cone, nitric acid, but are not oxidized by trifluoroperacetic acid.

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Russian Academy of Sciences
Russian Federation

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