Synthesis and crystal structural study of ternary molybdate NaMg3In(MoO4)5

descriptionPublicationkeyboard_double_arrow_right Article 01 Sep 1994 English Publisher:Springer Science and Business Media LLCJournal:Journal of Structural Chemistry, volume 34, pages 784-788 (issn: 0022-4766, eissn: 1573-8779,

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Authors: R. F. Klevtsova; A. D. Vasiliev; N. M. Kozhevnikova; L. A. Glinskaya; A. I. Kruglik; I. Yu. Kotova;

doi: 10.1007/bf00753580

Synthesis and crystal structural study of ternary molybdate NaMg3In(MoO4)5

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Abstract

We have synthesized single crystals of a temary molybdate NaMg3In(MoO4)5 and cam'ed out an X-ray structural study (a KM-4 automatic difiactometer, MoKα, radiation, 4503 F, R = 0.047). The triclinic unit cell dimensions are a = 7.0476(7), b = 17.935(2), c = 6.9849(7)A, α = 87.650(9), β= 100.980(8), ψ = 92.510(9)°, V= 865.5(2) A3, Z = 2, and space group P−1. The crystal structure involves MoO4 tetrahedra and (Mg, In)06 octahedra forming a three-dimensional framework with Na atoms located in its cavities. The compound melts at 990°C with decomposition.

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