Regioselectivity of the allylation of benzothiophene

descriptionPublicationkeyboard_double_arrow_right Article 01 Dec 1977 English Publisher:Springer Science and Business Media LLCJournal:Chemistry of Heterocyclic Compounds, volume 13, pages 1,296-1,298 (issn: 0009-3122, eissn: 1573-8353,

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Authors: A. V. Anisimov; Yu. N. Luzikov; V. M. Nikolaeva; Yu. N. Radyukin; �. A. Karakhanov; E. A. Viktorova;

doi: 10.1007/bf00469887

Regioselectivity of the allylation of benzothiophene

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Abstract

The reaction of benzothiophene with allyl halides in the presence of silver trichloroacetate in chlorine-containing hydrocarbons was investigated. It was established by gas-liquid chromatography and 13C NMR and mass spectrometry that 3-allylbenzothiophene and diallylbenzothiophene are formed in this case. The 13C NMR spectra were interpreted on the basis of an additive scheme with the utilization of benzothiophene, thiophene, and 2- and 3-allylthiophenes as models.

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Lomonosov Moscow State University
Russian Federation

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