A synthesis of the lactone of 5‐pyridoxic acid

descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 1959 English Publisher:WileyJournal:Recueil des Travaux Chimiques des Pays-Bas, volume 78, pages 244-246 (issn: 0165-0513, eissn: 0165-0513,

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Authors: H. M. Wuest; J. A. Bigot; Th. J. de Boer; B. V. D. Wal; J. P. Wibaut;

doi: 10.1002/recl.19590780403

A synthesis of the lactone of 5‐pyridoxic acid

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Abstract

AbstractThe reduction of dimethyl 2‐methyl‐3‐hydroxypyridine 4,5‐dicarboxylate (I) with sodium borohydride and aluminium chloride gives no pyridoxol but a precursor i.e. the lactone II, corresponding to 5‐pyridoxic acid. No isomeric lactone (III) corresponding to 4‐pyridoxic acid was isolated.

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