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image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Journal of the Ameri...arrow_drop_down
image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao
Journal of the American Pharmaceutical Association (Scientific ed )
Article . 1949 . Peer-reviewed
License: Elsevier TDM
Data sources: Crossref
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Sabadilla alkaloids. I. Extraction of total alkaloids

Authors: C E, POETSCH; L M, PARKS;

Sabadilla alkaloids. I. Extraction of total alkaloids

Abstract

A method is described by which the total sabadilla alkaloids were extracted from the seed and by which a partial separation of the crude alkaloidal mixture into four crude fractions was accomplished. Extraction of the seed with Skelly B removed the oil almost completely, in amounts up to 20 per cent, together with alkaloidal Fraction A, which was shaken out of the Skelly extract with acid. Extraction of the defatted seed with alcohol removed the remaining alkaloids. Concentration of this extract to a syrup and pouring into cold water yielded a precipitate of Fraction B which contained a considerable amount of alkaloid along with nonalkaloidal matter, probably resin. The filtrate from Fraction B, upon being made alkaline with ammonia, deposited Fraction C, which was removed by filtration. Chloroform extraction of the filtrate from C yielded Fraction D. From 15.5 Kg. of seed the following approximate amounts of the above fractions were obtained: A, 152 Gm.; B, 800 Gm.; C, 220 Gm.; D, 168 Gm.

Related Organizations
Keywords

Magnoliopsida, Alkaloids, Organic Chemicals

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
2
Average
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