Electrospray mass spectrometry of stable iminyl nitroxide and nitronyl nitroxide free radicals

descriptionPublicationkeyboard_double_arrow_right Article 13 Aug 2002 Australia English Publisher:WileyJournal:Journal of Mass Spectrometry, volume 37, pages 897-902 (issn: 1076-5174, eissn: 1096-9888,

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Authors: Smith, Craig; Bartley, John; Bottle, Steven;

doi: 10.1002/jms.339

pmid: 12271432

Electrospray mass spectrometry of stable iminyl nitroxide and nitronyl nitroxide free radicals

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Abstract

AbstractElectrospray ionization (ESI) mass spectra have been recorded for a range of substituted nitronyl nitroxide and iminyl nitroxide monoradicals and biradicals. Secondary species formed in the ESI source were observed as the dominant ions in both the iminyl nitroxide and nitronyl nitroxide spectra. Daughter ion spectrometry was used to establish fragmentation mechanisms for the nitronyl nitroxide and iminyl nitroxide moieties as well as the secondary species under ESI conditions. Copyright © 2002 John Wiley & Sons, Ltd.

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Australia

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Queensland University of Technology
Australia

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