Synthesis of novel 1,3‐substituted 1H‐[1,2,4]‐triazole‐3‐thiol derivatives

descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 2009 English Publisher:WileyJournal:Heteroatom Chemistry, volume 20, pages 405-410 (issn: 1042-7163, eissn: 1098-1071,

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Authors: Karine A. Eliazyan; Lusya V. Shahbazyan; Vergine A. Pivazyan; Emma A. Ghazaryan; Aleksandr P. Yengoyan;

doi: 10.1002/hc.20565

Synthesis of novel 1,3‐substituted 1H‐[1,2,4]‐triazole‐3‐thiol derivatives

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Abstract

AbstractBy means of regioselective S‐alkylation of 1H‐1,2,4‐triazole‐3‐thiol (1), a series of S‐substituted derivatives 2a‐j were synthesized. In certain conditions, the reaction of 2 with arylsulfochlorides, arylisocyanates, and quaternary ammonium salts of azines corresponding compounds were obtained 1‐arylsulfonyl‐ (3a‐d), 1‐arylcarbonamido‐ (4a,b), and 1‐azinyl‐1,2,4‐ (6a‐p) triazoles. Structures of compounds were confirmed by 1H NMR and elemental analyses. © 2010 Wiley Periodicals, Inc. Heteroatom Chem 20:405–410, 2009; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.20565

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