Facile Diastereoseparation of Glycosyl Sulfoxides by Chiral Stationary Phase

descriptionPublicationkeyboard_double_arrow_right Article 14 Jun 2016 English Publisher:WileyJournal:Chirality, volume 28, pages 534-539 (issn: 0899-0042, eissn: 1520-636X,

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Authors: Tohru, Taniguchi; Mai, Asahata; Akihito, Nasu; Yukatsu, Shichibu; Katsuaki, Konishi; Kenji, Monde;

doi: 10.1002/chir.22610

pmid: 27296702

Facile Diastereoseparation of Glycosyl Sulfoxides by Chiral Stationary Phase

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Abstract

AbstractSeparation of the diastereomers of glycosyl sulfoxides differing in the sulfur chirality has been difficult. This article presents a fast and scalable method for their diastereoseparation using a chiral stationary phase. The usefulness of this method was demonstrated in a 500‐mg scale separation within 20 min, and in the separation of trisaccharyl sulfoxide diastereomers. Chirality 28:534–539, 2016. © 2016 Wiley Periodicals, Inc.

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