Claisen–Schmidt Condensation Catalyzed by Metal‐Organic Frameworks

descriptionPublicationkeyboard_double_arrow_right Article 08 Mar 2010 English Publisher:WileyJournal:Advanced Synthesis & Catalysis, volume 352, pages 711-717 (issn: 1615-4150, eissn: 1615-4169,

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Authors: Amarajothi Dhakshinamoorthy; Mercedes Alvaro; Hermenegildo Garcia;

doi: 10.1002/adsc.200900747

Claisen–Schmidt Condensation Catalyzed by Metal‐Organic Frameworks

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Abstract

AbstractMetal‐organic framework [Fe(BTC) (BTC=1,3,5‐benzenetricarboxylic acid)] is a convenient heterogeneous catalyst for the carbon‐carbon bond forming reaction in toluene between acetophenone and benzaldehyde to give selectively chalcone in high yield. Fe(BTC) appears as a general catalyst able to synthesize selectively different chalcone derivatives bearing various functionalities. Fe(BTC) could be recycled with no significant loss of catalytic efficiency and crystallinity in subsequent runs.

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