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XRD datasets of B2N2-DBR (CCDC 2067979) and DBR (CCDC 2067980) compounds were collected on SPring-8 BL32XU using 0.7 Å wavelength with the EIGER X 9M detector (Dectris). Helical data collection scheme was used using 15×2 μm beam size and oscillation step of 0.2°. Diffraction images were indexed and integrated using DIALS, and scaled using XSCALE. BL32XU_DBR_multi.tar was not actually used, but collected for the test of multiple small wedge (10°/crystal) measurement for small molecules.
bl32xu, spring-8
bl32xu, spring-8
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