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Usos de Níquel Raney en síntesis orgánica

Authors: Ajoy K. Banerjee; Lisbeth Mendoza; Liadis Bedoya; Dioni Arrieche;

Usos de Níquel Raney en síntesis orgánica

Abstract

{"references": ["1. R. C. Norman en \"Principles of Organic Synthesis\" Mathum &CO Ltd, London, 1968, p.540 2. H. Adkins y H. R. Billica, J. Am. Chem. Soc., 70, 695 (1948). 3. T-K. Yang y D. S. Lee, en Encyclopedia of Reagents in Organic Synthesis, editor, L.A.Paquette, p4401 4. G. Pettit y E. E. van Tamelen, Org. Reactions, 12, 356 (1962). 5. H. Hauptmann y W. F.Walter, Chem. Rev. 62, 347 (1962). 6. L. Fieser, J. Am. Chem. Soc., 76, 1945 (1954). 7. D. Klass, M. Fieser y L. F. Fieser, J. Am. Chem. Soc., 77, 3829 (1955). 8. R. E. Ireland y P. W. Schiess, J. Org. Chem., 28, 23 (1963). 9. W. Reusch y D. Anderson, Tetrahedron, 22, 583 (1966). 10. C. Djerassi Y D. Williams, J. Chem. Soc., 4046 (1963). 11. J. L. Garc\u00eda Ruano, J. A.Fern\u00e1ndez-Salas, M. C. Maestro y A. Parra, Synthetic Communications, 43, 198 (2013). 12. R. Kronenthal y E. Becker, J. Am.Chem. Soc., 79, 1095 (1957). 13. J. A. Steele, L. A. Cohen y E. Mosettig, J. Am. Chem. Soc., 85, 1134 (1963). 14. M. E. Craft, W. J. Crooks III, B. Zorc y S. E. Milczanowski, J. Org. Chem., 53, 3158 (1988). 15. J. E. Taylor, Synthesis, 1142 (1985). 16. D. Monti, P. Gramatica, G. Speranza y P. Manitto, Tetrahedron Lett. 24, 417 (1983). 17. D. P. Curran, J. F. Brill Y D. M. Rakiewicz, J. Org. Chem., 49, 1654 (1984). 18. B. Staskum y T. Van Es, J. Chem. Soc.C., 531(1966). 19. Z. Sun, Z-H. Zhang, T-Q. Yuan, X. Ren and Z. Rong, ACS Catalysis, 11,10508 (2021). 20. H. O. House, Modern Synthetic Reactions; W. A. Benzamin: Menlo, CA 1972 y referencias relacionadas est\u00e1n citadas. 21. V. Georgian, R. Harrison y N. Gubish, J. Am. Chem. Soc., 81, 5834 (1959)."]}

Resumen Los diversos usos del catalizador Níquel Raney para la síntesis de compuestos orgánicos están ilustrados en este artículo. El uso principal de Níquel Raney en la desulfurización de tioacetales es bien conocido. Níquel Raney es un catalizador que está disponible comercialmente. El catalizador es pirofórico al contacto con el aire y por eso siempre se guarda en un solvente, comúnmente alcohólico.

Abstract The several uses of Raney nickel for the synthesis of organic compounds are described in this article. The principal use of Raney nickel for the desulfurization of thioketals is well known. Raney nickel is a commercially available catalyst. The catalyst ignites on contact with air and therefore it is most commonly kept in an alcoholic solvent.

Keywords

Desulfurización, Oxidación de alcoholes, Isomerización de cis-diol, Reducción de nitro alquenos.

1. R. C. Norman en “Principles of Organic Synthesis” Mathum &CO Ltd, London, 1968, p.540 2. H. Adkins y H. R. Billica, J. Am. Chem. Soc., 70, 695 (1948). 3. T-K. Yang y D. S. Lee, en Encyclopedia of Reagents in Organic Synthesis, editor, L.A.Paquette, p4401 4. G. Pettit y E. E. van Tamelen, Org. Reactions, 12, 356 (1962). 5. H. Hauptmann y W. F.Walter, Chem. Rev. 62, 347 (1962).

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