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image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Thermochimica Actaarrow_drop_down
image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao
Thermochimica Acta
Article . 2012 . Peer-reviewed
License: Elsevier TDM
Data sources: Crossref
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Thermal lag analysis on a simulated TGA-DSC device

Authors: Roberto Comesaña; Miguel A. Gómez; Miguel A. Álvarez; Pablo Eguía;

Thermal lag analysis on a simulated TGA-DSC device

Abstract

Abstract A ThermoGravimetric Analyser with Differential Scanning Calorimeter (TGA-DSC) has been simulated to evaluate the influence of different parameters on thermal lag. Two virtual materials with selected properties were created and combined with two heating rates. A three-dimensional mesh was created based on measurements in the actual TGA-DSC. Specific models have been applied and boundary conditions have been configured, including a programmed Proportional Integral Derivative (PID) controller to regulate temperature. The results showed that a sample with a lower thermal diffusivity had greater temperature differences when compared to the furnace temperature than a sample with a higher thermal diffusivity. Biot number has also been computed to analyse temperature differences within the sample. Thermal diffusivity and Biot number effects were miniscule compared to the heating rate, which increased sample temperature instability and temperature differences within the sample.

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
30
Top 10%
Top 10%
Average
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