
handle: 2318/93166
By means of in situ synchrotron radiation powder X-ray diffraction, powder neutron diffraction, attenuated total reflectance infrared spectroscopy, differential scanning calorimetry and the Sieverts techniques we have investigated how anion substitution in the LiBH4eLiBr system leads to changes in the structural, physical, chemical and hydrogen storage properties of this material. Mechano-chemical treatment facilitates formation of a hexagonal solid solution h-Li(BH4)1� xBrx whereas heating at elevated temperatures, i.e. T > 112
Lithium borohydride, Sieverts method, In situ powder X-ray diffraction, Hydrogen storage, Infrared spectroscopy, Anion substitution
Lithium borohydride, Sieverts method, In situ powder X-ray diffraction, Hydrogen storage, Infrared spectroscopy, Anion substitution
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