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Journal of Sol-Gel Science and Technology; ZENODO
Other literature type . Article . 2019 . Peer-reviewed
License: Springer TDM
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Novel synthetic approach to the preparation of single-phase BixLa1−xMnO3+δ solid solutions

Authors: Dovydas Karoblis; Kestutis Mazeika; Dalis Baltrunas; Anna Lukowiak; Wieslaw Strek; Aleksej Zarkov; Aivaras Kareiva;

Novel synthetic approach to the preparation of single-phase BixLa1−xMnO3+δ solid solutions

Abstract

In this study, the BixLa1−xMnO3+δ solid solutions (x from 0 to 0.65) were synthesized using sol–gel combustion method with citric acid as a fuel and complexing agent. It was shown that changes in chemical composition of the materials lead to the evolution of crystal structure, morphology, and magnetic properties. The thermal behavior of precursor gel was investigated by thermogravimetric and differential scanning calorimetry (TG-DSC) measurements. X-ray diffraction (XRD) analysis demonstrated that all samples were monophasic. The Rietveld analysis showed that the structure can be indexed by trigonal or cubic unit cell depending on Bi3+ content. Scanning electron microscopy (SEM) was used to evaluate morphological features of the synthesized materials and revealed that Bi3+ ions significantly promote growth of the grains. The sol–gel-derived BixLa1−xMnO3+δ specimens were also characterized by FT-IR spectroscopy and magnetization measurements, which showed a clear correlation between magnetic properties and crystal structure of the materials.

Subjects by Vocabulary

Microsoft Academic Graph classification: Thermogravimetric analysis Materials science Scanning electron microscope Analytical chemistry Crystal structure Magnetization Differential scanning calorimetry Spectroscopy Rietveld refinement Solid solution

Keywords

Sol-gel processing, Biomaterials, Materials Chemistry, Bismuth manganite, General Chemistry, Condensed Matter Physics, Electronic, Optical and Magnetic Materials, Paramagnetic, Ceramics and Composites

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    popularity
    This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
    Top 10%
    influence
    This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
    Average
    impulse
    This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
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download
citations
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
views
OpenAIRE UsageCountsViews provided by UsageCounts
downloads
OpenAIRE UsageCountsDownloads provided by UsageCounts
10
Top 10%
Average
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57
81
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