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image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Journal of Pharmaceu...arrow_drop_down
image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao
Journal of Pharmaceutical Sciences
Article . 1966 . Peer-reviewed
License: Elsevier TDM
Data sources: Crossref
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Evaluation of Automatic Potentiometric Titrator in Nonaqueous Titrations

Authors: T, Medwick; E, Kirschner;

Evaluation of Automatic Potentiometric Titrator in Nonaqueous Titrations

Abstract

A procedure is reported for the evaluation of the behavior of an automatic recording titrator in nonaqueous titrations and is applied to an instrument composed of commercially available units. First, the behavior of the purely instrumental features was determined and the experimental errors were compared with calculated maximum anticipated relative values. The instrument's function in this case was within expectation. Then, the response of the titrator was evaluated from titration curve properties of two compounds in acetic acid and two other compounds in iso-propanol. The following maximum relative errors, with instrumental errors discounted, were observed: range, 1.5 per cent; end point potential, 4.4 per cent; analytical results, 1.0 per cent; slope of the rapidly rising portion, 11.4 per cent. On the basis of satisfactory instrumental response and reasonable titration curve errors, the relatively inexpensive unit used here is found reliable for general laboratory use. The procedure described is recommended for use in evaluating any automatic potentiometric recorder.

Related Organizations
Keywords

Evaluation Studies as Topic, Potentiometry, Benzoates, Guanidines, Nitrobenzenes

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
5
Average
Top 10%
Average
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