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Hydride Reduction by a Sodium Hydride–Iodide Composite

descriptionPublicationkeyboard_double_arrow_right Article 16 Feb 2016 Singapore English Publisher:WileyJournal:Angewandte Chemie, volume 128, pages 3,783-3,787 (issn: 0044-8249, eissn: 1521-3757, Copyright policy )
Authors: Too, Pei Chui; Chan, Guo Hao; Tnay, Ya Lin; Hirao, Hajime; Chiba, Shunsuke;

doi: 10.1002/ange.201600305 , 10.1002/anie.201600305

pmid: 26878823

pmc: PMC4797714

Hydride Reduction by a Sodium Hydride–Iodide Composite

Abstract

AbstractSodium hydride (NaH) is widely used as a Brønsted base in chemical synthesis and reacts with various Brønsted acids, whereas it rarely behaves as a reducing reagent through delivery of the hydride to polar π electrophiles. This study presents a series of reduction reactions of nitriles, amides, and imines as enabled by NaH in the presence of LiI or NaI. This remarkably simple protocol endows NaH with unprecedented and unique hydride‐donor chemical reactivity.

Country
Singapore
Related Organizations
Keywords

Sodium hydride, Decyanation, Communications

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    influence
    This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
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    This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
79
Top 10%
Top 10%
Top 1%
Green
hybrid