publication . Article . Preprint . Other literature type . 2017

On the origin of surface imposed anisotropic growth of salicylic and acetylsalicylic acids crystals during droplet evaporation

Maciej Przybyłek; Dorota Ziółkowska;
Open Access
  • Published: 25 Jul 2017
  • Country: France
Abstract
International audience; In this paper droplet evaporative crystallization of salicylic acid (SA) and acetylsalicylic acid (ASA) crystals on different surfaces, such as glass, polyvinyl alcohol (PVA), and paraffin was studied. The obtained crystals were analyzed using powder X-ray diffraction (PXRD) technique. In order to better understand the effect of the surface on evaporative crystallization, crystals deposited on glass were scraped off. Moreover, evaporative crystallization of a large volume of solution was performed. As we found, paraffin which is non-polar surface promotes formation of crystals morphologically similar to those obtained via bulk evaporative...
Subjects
free text keywords: 30301 Chemical Characterisation of Materials, Computational Chemistry, Crystallography, 30302 Nanochemistry and Supramolecular Chemistry, 30304 Physical Chemistry of Materials, 30701 Quantum Chemistry, 30206 Solid State Chemistry, 30606 Structural Chemistry and Spectroscopy, Supramolecular Chemistry, 30306 Synthesis of Materials, 30307 Theory and Design of Materials, 30799 Theoretical and Computational Chemistry not elsewhere classified, 30602 Chemical Thermodynamics and Energetics, FOS: Chemical sciences, Acetylsalicylic acid, Crystal morphology, Droplet evaporative crystallization, Intermolecular interactions, Powder x-ray diffraction, Salicylic acid, [CHIM.CRIS]Chemical Sciences/Cristallography, Physics - Chemical Physics, [ CHIM.CRIS ] Chemical Sciences/Cristallography, Original Paper, Physical and Theoretical Chemistry, Inorganic Chemistry, Organic Chemistry, Computational Theory and Mathematics, Catalysis, Computer Science Applications
94 references, page 1 of 7

1. Lemke TL, Williams DA (2008) Foye's principles of medicinal chemistry. Kluwer, Baltimore

2. Patrick GL (1995) An introduction to medicinal chemistry. Oxford University Press, Oxford

3. Ahluwalia VK, Bhagat P, Aggarwal R, Chandra R (2005) Intermediate for organic synthesis. I. K. International Pvt. Ltd, New Delhi

4. Singh YP, Das R, Singh RA (2007) Numerical simulation of the internal vibrations of COOH group in amino-salicylic acids. Afr J Biochem Res 1:019-023

5. Wen P, Chen J, Wan S, Kong W, Zhang P, Wang W, Zhan J, Pan Q, Huang W (2008) Salicylic acid activates phenylalanine ammonialyase in grape berry in response to high temperature stress. Plant Growth Regul 55:1-10. doi:10.1007/s10725-007-9250-7

6. Elbagerma MA, Edwards HG, Munshi T, Scowen IJ (2010) Identification of a new co-crystal of salicylic acid and benzamide of pharmaceutical relevance. Anal Bioanal 397:137-146. doi:10. 1007/s00216-009-3375-7

7. Trask AV, Jones W (2005) Crystal engineering of organic cocrystals by the solid-state grinding approach. Top Curr Chem 254:41-70. doi: 10.1007/b100995

8. Kastelic J, Lah N, Kikelj D, Leban I (2011) A 1:1 co-crystal of fluconazole with salicylic acid. Acta Cryst C 67:370-372. doi:10. 1107/S0108270111031155 [OpenAIRE]

9. Aitipamula S, Wong ABH, Chow PS, Tan RBH (2012) Pharmaceutical cocrystals of ethenzamide: structural, solubility and dissolution studies. Cryst Eng Comm 14:8515-8524. doi:10.1039/ C2CE26325D

10. Kumar A, Sahoo SK, Padhee K, Kochar PS, Sathapathy A, Pathak N (2011) Review on solubility enhancement techniques for hydrophobic drugs. Pharmacie Globale 3:001-007

11. Derle D, Patel J, Yeole D, Patel A, Pingle A (2010) Particle engineering techniques to enhance dissolution of poorly water soluble drugs. International J Current Pharm Res 2:10-15

12. Chaudhary A, Nagaich U, Gulati N, Sharma V, Khosa R, Partapur MUP (2012) Enhancement of solubilization and bioavailability of poorly soluble drugs by physical and chemical modifications: a recent review. J Adv Pharm Educ Res 2:32-67

13. Lonare AA, Patel SR (2013) Antisolvent crystallization of poorly water soluble drugs. Int J Chem Eng Appl 4:337-341

14. Purvis T, Mattucci ME, Crisp MT, Johnston KP, Williams RO (2007) Rapidly dissolving repaglinide powders produced by the ultra-rapid freezing process. AAPS Pharm Sci Tech 8:E1-E9. doi:10.1208/ pt0803058

15. Rogers TL, Overhoff KA, Shah P, Santiago P, Yacaman MJ, Johnston KP, Williams RO III (2003) Micronized powders of a poorly water soluble drug produced by a spray-freezing into liquid-emulsion process. Eur J Pharm Biopharm 55:161-172. doi:10.1016/S0939- 6411(02)00193-5

94 references, page 1 of 7
Abstract
International audience; In this paper droplet evaporative crystallization of salicylic acid (SA) and acetylsalicylic acid (ASA) crystals on different surfaces, such as glass, polyvinyl alcohol (PVA), and paraffin was studied. The obtained crystals were analyzed using powder X-ray diffraction (PXRD) technique. In order to better understand the effect of the surface on evaporative crystallization, crystals deposited on glass were scraped off. Moreover, evaporative crystallization of a large volume of solution was performed. As we found, paraffin which is non-polar surface promotes formation of crystals morphologically similar to those obtained via bulk evaporative...
Subjects
free text keywords: 30301 Chemical Characterisation of Materials, Computational Chemistry, Crystallography, 30302 Nanochemistry and Supramolecular Chemistry, 30304 Physical Chemistry of Materials, 30701 Quantum Chemistry, 30206 Solid State Chemistry, 30606 Structural Chemistry and Spectroscopy, Supramolecular Chemistry, 30306 Synthesis of Materials, 30307 Theory and Design of Materials, 30799 Theoretical and Computational Chemistry not elsewhere classified, 30602 Chemical Thermodynamics and Energetics, FOS: Chemical sciences, Acetylsalicylic acid, Crystal morphology, Droplet evaporative crystallization, Intermolecular interactions, Powder x-ray diffraction, Salicylic acid, [CHIM.CRIS]Chemical Sciences/Cristallography, Physics - Chemical Physics, [ CHIM.CRIS ] Chemical Sciences/Cristallography, Original Paper, Physical and Theoretical Chemistry, Inorganic Chemistry, Organic Chemistry, Computational Theory and Mathematics, Catalysis, Computer Science Applications
94 references, page 1 of 7

1. Lemke TL, Williams DA (2008) Foye's principles of medicinal chemistry. Kluwer, Baltimore

2. Patrick GL (1995) An introduction to medicinal chemistry. Oxford University Press, Oxford

3. Ahluwalia VK, Bhagat P, Aggarwal R, Chandra R (2005) Intermediate for organic synthesis. I. K. International Pvt. Ltd, New Delhi

4. Singh YP, Das R, Singh RA (2007) Numerical simulation of the internal vibrations of COOH group in amino-salicylic acids. Afr J Biochem Res 1:019-023

5. Wen P, Chen J, Wan S, Kong W, Zhang P, Wang W, Zhan J, Pan Q, Huang W (2008) Salicylic acid activates phenylalanine ammonialyase in grape berry in response to high temperature stress. Plant Growth Regul 55:1-10. doi:10.1007/s10725-007-9250-7

6. Elbagerma MA, Edwards HG, Munshi T, Scowen IJ (2010) Identification of a new co-crystal of salicylic acid and benzamide of pharmaceutical relevance. Anal Bioanal 397:137-146. doi:10. 1007/s00216-009-3375-7

7. Trask AV, Jones W (2005) Crystal engineering of organic cocrystals by the solid-state grinding approach. Top Curr Chem 254:41-70. doi: 10.1007/b100995

8. Kastelic J, Lah N, Kikelj D, Leban I (2011) A 1:1 co-crystal of fluconazole with salicylic acid. Acta Cryst C 67:370-372. doi:10. 1107/S0108270111031155 [OpenAIRE]

9. Aitipamula S, Wong ABH, Chow PS, Tan RBH (2012) Pharmaceutical cocrystals of ethenzamide: structural, solubility and dissolution studies. Cryst Eng Comm 14:8515-8524. doi:10.1039/ C2CE26325D

10. Kumar A, Sahoo SK, Padhee K, Kochar PS, Sathapathy A, Pathak N (2011) Review on solubility enhancement techniques for hydrophobic drugs. Pharmacie Globale 3:001-007

11. Derle D, Patel J, Yeole D, Patel A, Pingle A (2010) Particle engineering techniques to enhance dissolution of poorly water soluble drugs. International J Current Pharm Res 2:10-15

12. Chaudhary A, Nagaich U, Gulati N, Sharma V, Khosa R, Partapur MUP (2012) Enhancement of solubilization and bioavailability of poorly soluble drugs by physical and chemical modifications: a recent review. J Adv Pharm Educ Res 2:32-67

13. Lonare AA, Patel SR (2013) Antisolvent crystallization of poorly water soluble drugs. Int J Chem Eng Appl 4:337-341

14. Purvis T, Mattucci ME, Crisp MT, Johnston KP, Williams RO (2007) Rapidly dissolving repaglinide powders produced by the ultra-rapid freezing process. AAPS Pharm Sci Tech 8:E1-E9. doi:10.1208/ pt0803058

15. Rogers TL, Overhoff KA, Shah P, Santiago P, Yacaman MJ, Johnston KP, Williams RO III (2003) Micronized powders of a poorly water soluble drug produced by a spray-freezing into liquid-emulsion process. Eur J Pharm Biopharm 55:161-172. doi:10.1016/S0939- 6411(02)00193-5

94 references, page 1 of 7
Powered by OpenAIRE Research Graph
Any information missing or wrong?Report an Issue