publication . Doctoral thesis . 2010

On new allotropes and nanostructures of carbon nitrides

Bojdys, Michael Janus;
Open Access English
  • Published: 22 Feb 2010
  • Country: Germany
Abstract
In the first section of the thesis graphitic carbon nitride was for the first time synthesised using the high-temperature condensation of dicyandiamide (DCDA) – a simple molecular precursor – in a eutectic salt melt of lithium chloride and potassium chloride. The extent of condensation, namely next to complete conversion of all reactive end groups, was verified by elemental microanalysis and vibrational spectroscopy. TEM- and SEM-measurements gave detailed insight into the well-defined morphology of these organic crystals, which are not based on 0D or 1D constituents like known molecular or short-chain polymeric crystals but on the packing motif of extended 2D f...
Subjects
free text keywords: Institut für Chemie, Extern, ddc:540
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