publication . Article . 2013

Preparation and characterization of sodium dodecyl sulfate doped polypyrrole solid phase micro extraction fiber and its application to endocrine disruptor pesticide analysis

Korba, Korcan; Pelit, Levent; Pelit, Fusun Okcu; Ozdokur, K. Volkan; Ertas, Hasan; Eroglu, Ahmet E.; Ertas, F. Nil;
Open Access English
  • Published: 01 Jun 2013
  • Publisher: Elsevier
Abstract
A robust in house solid-phase micro extraction (SPME) surface has been developed for the headspace (HS)-SPME determination of endocrine disruptor pesticides, namely, Chlorpyrifos, Penconazole, Procymidone, Bromopropylate and Lambda-Cyhalothrin in wine sample by using sodium dodecylsulfate doped polypyrrole SPME fiber. Pyrrole monomer was electrochemically polymerized on a stainless steel wire in laboratory conditions in virtue of diminishing the cost and enhancing the analyte retention on its surface to exert better selectivity and hence the developed polymerized surface could offer to analyst to exploit it as a fiber in headspace SPME analysis. The parameters, ...
Subjects
free text keywords: Head space solid phase micro extraction, Red wine, Endocrine disruptor pesticide, Polypyrrole fiber, Extraction, Gas chromatography
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publication . Article . 2013

Preparation and characterization of sodium dodecyl sulfate doped polypyrrole solid phase micro extraction fiber and its application to endocrine disruptor pesticide analysis

Korba, Korcan; Pelit, Levent; Pelit, Fusun Okcu; Ozdokur, K. Volkan; Ertas, Hasan; Eroglu, Ahmet E.; Ertas, F. Nil;