publication . Article . 2013

Qualitative and Quantitative Control of Honeys Using NMR Spectroscopy and Chemometrics

Marc Ohmenhaeuser; Yulia B. Monakhova; Thomas Kuballa; Dirk W. Lachenmeier;
Open Access
  • Published: 16 Apr 2013 Journal: ISRN Analytical Chemistry, volume 2,013, pages 1-9 (eissn: 2090-732X, Copyright policy)
  • Publisher: Hindawi Limited
<jats:p>400 MHz nuclear magnetic resonance (NMR) spectroscopy and multivariate data analysis techniques were used in the context of food surveillance to measure 328 honey samples with<jats:sup>1</jats:sup>H and<jats:sup>13</jats:sup>C NMR. Using principal component analysis (PCA), clusters of honeys from the same botanical origin were observed. The chemical shifts of the principal monosaccharides (glucose and fructose) were found to be mostly responsible for this differentiation. Furthermore, soft independent modeling of class analogy (SIMCA) and partial least squares discriminant analysis (PLS-DA) could be used to automatically classify spectra according to the...
free text keywords: honey, authenticity, NMR, Article Subject
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