A Protocol for the exo-Mono and exo,exo-Bis Functionalization of the Diazocine Ring of Tröger’s Base

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Dawaigher, Sami; Månsson, Kristoffer; Ascic, Erhad; Artacho, Josep; Mårtensson, Roger; Loganathan, Nagarajan; Wendt, Ola F.; Harmata, Michael; Snieckus, Victor; Wärnmark, Kenneth;
(2015)
  • Publisher: Figshare
  • Related identifiers: doi: 10.1021/acs.joc.5b01921.s002, doi: 10.1021/acs.joc.5b01921.s001
  • Subject: Biotechnology | Developmental Biology | benzylic 6 | Physiology | electrophile | Plant Biology | Tro | 12 positions | diazocine ring | Biochemistry | Biophysics | exo
    • FOR: 59999 Environmental Sciences not elsewhere classified | 110309 Infectious Diseases | 69999 Biological Sciences not elsewhere classified | 60506 Virology | 39999 Chemical Sciences not elsewhere classified

An efficient protocol has been developed for the <i>exo-</i>mono and <i>exo</i>,<i>exo</i>-bis functionalization of Tröger’s base in the benzylic 6 and 12 positions of the diazocine ring. The lithiation of Tröger’s base using <i>s</i>-BuLi/TMEDA followed b... View more
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