Rare-Earth Metalation of Calix[4]pyrrole/Calix[4]arene Free of Alkali-Metal Companions

Deacon, Glen B.; Gardiner, Michael G.; Junk, Peter C.; Townley, Josh P.; Wang, Jun;

The redox transmetalation/protolysis (RTP) reactions of ytterbium or neodymium metal with calix[4]­H<sub>4</sub> (5,11,17,23-tetra-<i>tert</i>-butylcalix­[4]­arene-25,26,27,28-tetrol) in the presence of bis­(pentafluorophenyl)mercury under ultrasonication yield... View more
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