Radical Hydroxyalkylation of C−H Bond Adjacent to Nitrogen of Tertiary Amides, Ureas, and Amines

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Yoshimitsu, Takehiko; Arano, Yoshimasa; Nagaoka, Hiroto;
(2005)

Tertiary amides, ureas, and amines undergo direct intermolecular addition to aldehydes under the Et<sub>3</sub>B/air conditions, thereby providing a unique and simple means for the radical sp<sup>3</sup> C−H transformation of nitrogen-containing molecules.
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