Solid-State 15N CPMAS NMR and Computational Analysis of Ligand Hapticity in Rhodium(η-diene) Poly(pyrazolyl)borate Complexes

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Pettinari, Riccardo; Pettinari, Claudio; Marchetti, Fabio; Gobetto, Roberto; Nervi, Carlo; Chierotti, Michele R.; Chan, Eric J.; Skelton, Brian W.; White, Allan H.;
(2010)
  • Publisher: Figshare
  • Related identifiers: doi: 10.1021/ic101830e.s004, doi: 10.1021/ic101830e.s003, doi: 10.1021/ic101830e.s006, doi: 10.1021/ic101830e.s005, doi: 10.1021/ic101830e.s002, doi: 10.1021/ic101830e.s001
  • Subject: Tpx ligands | Tp 4Bo diene | Rh metal | κ2 ligands | Plant Biology | 13 C NMR solution | spectroscopic data | hydrotri | Space Science | Genetics | Pharmacology | Low steric hindrance | Computational Analysis | Biophysics | 15 N chemical shifts | Ligand Hapticity | Inorganic Chemistry | steric encumbrance | Tpa | 15 N CPMAS studies | Rh complexes | IR | Medicine | κ3 coordination | Computational Biology | coordination modes | nbd | Hematology | 11 B | Tp 4Bo | Biochemistry | 1 H
    • FOR: 80699 Information Systems not elsewhere classified | 29999 Physical Sciences not elsewhere classified | 69999 Biological Sciences not elsewhere classified | 39999 Chemical Sciences not elsewhere classified
    acm: TheoryofComputation_ANALYSISOFALGORITHMSANDPROBLEMCOMPLEXITY

Novel [Rh(η-diene)Tp<sup>x</sup>] complexes of sterically encumbered Tp<sup>x</sup> ligands (Tp<sup>x</sup> = Tp<sup>4Bo</sup>, diene = cod, <b>1</b>; nbd, <b>2</b>; Tp<sup>x</sup> = Tp<sup>4Bo,5Me</sup>, diene = cod, <b>3</b>; nbd, <b>4</b>; Tp<sup>x</sup> = Tp<sup>a,3... View more
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